Thermogravimetry "Jupiter"

Catalysis on Metals group

STA 449 Jupiter thermoanalyser (Netzsch) for simultaneous thermal analysis to 1500 °C , equipped with the pulse box for PulseTA and coupled with a quadrupole mass spectrometer for monitoring the composition of the gas phase

Temperature range                       RT - +1100 °C
Heating rate                                   0.1 - 50 Kpm
Pressure     1 bar/3 mbar
Sample                             max 40-85 ul, 0.2 ml
Available Gases                             Ar, O₂, H₂, N₂O
Methods                                         TG, DSC, DTA, Pulse TA
Gas phase analysis                   QMS

Tarasov, A.; Schumann, J.; Girgsdies, F.; Thomas, N.; Behrens, M.: Thermokinetic investigation of binary Cu/Zn hydroxycarbonates as precursors for Cu/ZnO catalysts. Thermochimica Acta 591, pp. 1 - 9 (2014)

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Schumann, J.; Tarasov, A.; Thomas, N.; Schlögl, R.; Behrens, M.: Cu,Zn-based catalysts for methanol synthesis: On the effect of calcination conditions and the part of residual carbonates. Applied Catalysis A 516, pp. 117 - 126 (2016)

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Millet, M.-M.; Frei, E.; Algara-Siller, G.; Schlögl, R.; Tarasova, A.: Surface titration of supported Ni catalysts by O2-pulse thermal analysis. Applied Catalysis A: General (566), pp. 155 - 163 (2018)

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Willinger, E.; Massué, C.; Schlögl, R.; Willinger, M. G.: Identifying key structural features of IrOx water splitting catalysts. Journal of the American Chemical Society 139 (34), pp. 12093 - 12101 (2017)

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supplementary-material